• Proton Nuclear Magnetic Resonance

• Process your data automatically (1H, 13C, DEPTs or any other 1D NMR as well as any 2D NMR correlations, such as HSQC, HMBC, NOESY, COSY, TOCSY, etc.).
• Delta Software For Nmr Spectroscopy. Haward Technology has delivered internationally-accredited courses for major oil and gas, power and process companies through its.

Delta Software For Nmr Database. An NMR and Mass Spectroscopy. The ECX NMR system is controlled by the JEOL Delta NMR software package.

Mass Spectrometry – JEOL’s high resolution mass spectrometers are used to accurately identify the chemical composition and the structure of molecules in substances, and to analyze chemical reactions. From characterization of unknown chemical structures using LC or GC (liquid or gas chromatography) to instantaneous detection of counterfeit drugs or environmental toxins using revolutionary open air mass spectrometry (DART), JEOL mass spectrometers serve science and research in many impactful ways every day. Direct Analysis in Real Time (DART) – Developed in 2003, has completely revolutionized mass spectrometry.

For the first time in the history of mass spec, researchers can analyze the chemical composition of samples without sample alteration, in an open air environment. The AccuTOF-DART has gained rapid acceptance at pharmaceutical companies, universities, homeland security sites, and world class forensics labs. Nuclear Magnetic Resonance (NMR) Spectroscopy – The JEOL NMR offers unique advantages in the study of both small and large molecules and their chemical structures using 1D, 2D, 3D, and solid state spectroscopy.

NMR experiments are made simpler through automated functions, including gradient shimming, variable temperature control, and sample exchange. NMR & Mass Spec – A novel concept: NMR experiments combined with DART open air mass spectrometry to instantly acquire mass spectra of a sample in an NMR tube, without further sample preparation. Unbeatable productivity and turnaround time for students and universities, and for busy labs.

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The Department of Chemistry and Biochemistry has excellent NMR facilities to support its teaching and research programs. A JEOL ECA 500 MHz spectrometer and a JEOL ECS 400 MHz spectrometer are housed at the Patricia Sullivan Science Building in Room 001.

Proton Nuclear Magnetic Resonance

The JEOL 500 is built on a 12 T Oxford standard bore magnet and the JEOL 400 on a 9.6 T Jastech magnet. The JEOL ECA 500 NMR Spectrometer contains a 5 mm tunable PFG probe designed with an outer high frequency coil for 1H and 19F observation and an inner tunable low frequency coil for observation of nuclei including 13C, 15N, 31P, and other esoteric nuclei. The spectrometer contains a Z-axis pulse field gradient system that can operate at 30 G/cm. Gradient shimming makes for convenient operation at high homogeneity. 1-D and 2-D experiments are convenient for both experienced and novice NMR operators using DELTA software with programmed routines including 1-D experiments for a multitude of nuclei as well as COSY, NOESY, HMQC, HMBC, DEPT, HETCOR, HSQC, INEPT, ROESY AND TOCSY. The JEOL ECS 400, our newest spectrometer, has all the capabilities of the JEOL 500 and additionally is equipped with a high sensitivity JEOL Royal probe plus an NMR 24-position sample changer.